monoclinic相关论文
The temporal evolution of domain structure and its piezoelectric behavior of ferroelectric material BaTiO3 during the tr......
Simple Preparation of LaPO4:Ce, Tb Phosphors by an Ionic--Liquid--Driven Supported Liquid Membrane S
In this work, LaPO_4:Ce, Tb phosphors were prepared by firing a LaPO_4:Ce, Tb precipitate using an ionic-liquid-driven s......
用电子束蒸发沉积在K9玻璃基底上镀制HfO2薄膜,沉积温度为200℃,蒸发速率为0.03nm/s。由X射线衍射谱可知薄膜出现明显结晶,且为单......
Coordination compounds of lanthanide trichloroacetates with 1,10-phenanthroline weresynthesized and characterized as Ln......
The title complex L3Y(L = [O-4,6-di-tBu-C6H2-2-CH{CH(iPr2NCHCHN) }]) has been synthesized by the reaction of LiY[N(iPr) ......
A new hexanuclear silver(I) compound containing thiosemicarbazones with groups of 1-naphthalene was synthesized and stru......
ZrOCl2·8H2O and ZrO(NO3)2·2H2O were used respectively to synthesize a NASICON solid electrolyte by a sol-gel method. T......
Solid-state phase transitions of 4-methylanilinium perchlorate (4-CH 3 C 6 H 4 NH 3 ·ClO 4 , 1) and tetrafluoroborate (......
The structures and thermal expansion properties of Lu2-xFexMo3O12 have been investigated by X-ray diffraction(XRD).XRD p......
Effect of alcohol solvents treated ZrO(OH)_2 hydrogel on properties of ZrO_2 and its catalytic perfo
A series of ZrO2 catalysts were prepared by treating ZrO(OH)2 hydrogel with different alcohol solvents (C2-C4 alcohols) ......
Two new hydrazone compounds, 3-bromo-N’-(2-chloro-5-nitrobenzylidene)-ben- zohydrazide 1 and 3-bromo-N’-(4-nitrobenzyl......
A new asymmetric bidentate copper(Ⅱ) complex,CuL 2(HL=2-((E)-(4-bromophenylimino)methyl)-6-bromo-4-chlorophenol),has be......
Synthesis, Crystal Structure and Antitumor Activity of 6,7,8-Trimethoxy-1-(4-methoxy-3-nitrophenyl)-
A novel class of 3,4-dihydroisoquinolines (7a~e) was designed, synthesized and characterized by IR, NMR and ESI-MS. The c......
SOFC composite electrolyte based on LSGM-8282 and zirconia or doped zirconia from zircon concentrate
The aim of this research is to study zirconia-based electrolyte materials to increase the commercial value of zircon con......
Two-dimensional Lanthanide Coordination Polymers Constructed from Ce~3+/Pr~3+ Cation,Imidazole-4,5-d
Two new lanthanide coordination polymers [Ln(C 5 H 2 N 2 O 4)(H 2 O) 2 (C 2 O 4) 0.5 ] n nH 2 O (Ln=Ce III (1) or Pr III......
One novel entangled cobalt compound,{[Co 3 (nbta) 2 (4,4-bpy) 2 (H 2 O) 2 ](H 2 O) 2 } n (1,H 3 nbta=5-nitro-1,2,3-benze......
Synthesis, Crystal Structure and Photocatalytic Properties of a Supramolecular Assembly Based on Keg
A new supramolecular compound (4,4’-bipyH)4[SiW12O40](4,4’-bipy) (4,4’-bipy = 4,4’-bipyridine) was synthesized hydro......
Preparation and morphology of nano-size ceria by a stripping precipitation using oxalic acid as a pr
The precursors organic cerium deposits were obtained by a stripping precipitation method from cerium-loaded P507 organic......
A new crystal of N,N’-bis(4-nitrophenylcarbamothioyl)isophthalamide DMF solva-te has been prepared at room temperature ......
Synthesis and Crystal Structure of a New Mn(Ⅱ) Coordination Polymer Based on Asymmetric Semi-rigid V
A novel manganese(Ⅱ) coordination polymer with 2-(4-carboxyphenoxy) benzoic acid (2,4’-H2oba) and 1,10-phenanthroline ......
Synthesis and Crystal Structure of(E)-Ethyl 2-(5-(3-methyl-2-butenyloxy)-2-(3-(4-(3-methyl-2-butenyl
The title compound,(E)-ethyl 2-(5-(3-methyl-2-butenyloxy)-2-(3-(4-(3-methyl-2-butenyloxy)phenyl) acryloyl) phenoxy)aceta......
A new tri-nuclear mixed metal thiolate complex [Ag(PPh3)2]2[Ni(edtO2)2] 1 has been synthesized and structurally characte......
A Novel Copper(II) Coordination Polymer with Figure-of-eight-shaped Channels Occupied by Flexible Mo
A copper(II) coordination polymer, [Cu3(HOA)2(bpp)4]n (1, H4OA = 3,3′,4,4′-oxidiphthalic acid, bpp = 1,3-bis(4-pyridyl......
Synthesis and Structure of bc-Dichloro-af-dihydroxo-de-bis(N-3-pyridinylmethanesulfonamide)platinum(
The Pt(Ⅳ) complex cis,cis,trans-[Pt(PMSA)2Cl2(OH)2]2H2O (1), where PMSA=N-3-pyridinylmethanesulfonamide, has been synth......
An Unusual Binodal (4,12)-Connected 3D Supramolecular Network Based on [Mn_4(OH)_2(H_2O)_2]~(6+) Sub
A new two-dimensional MnⅡ metal-organic framework (MOF), [Mn4(μ3-OH)2L2 (4,4 -bipy)2(H2O)2]·H2O(1, H3 L= 5-oxyacetate......
The title compound N-(2,6-difluorobenzoyl)-N’-[5-(4-trifluoromethylphenyl)-1,3,4-thiadiazol-2-yl]urea(C17H9F5N4O2S,Mr =......
Synthesis,Structure and Thermal Stability of a Cadmium Coordination Polymer:[Cd(phen)(4,6-dimethyl-5
One cadmium(Ⅱ)coordination polymer [Cd(phen)(4,6-dimethyl-5-nitro-isophtha-lic acid)]n(1)has been synthesized with 4,6-......
Under hydrothermal conditions, 4-(4,5-dicarboxy-1H-imidazol-2-yl)pyridine 1-oxide (H3DCImPyO) reacted with ZnCl2 to give......
A novel coordination complex [Zn(bipy)2(H2O)4]·L·3H2O (1, bipy = 4,4’-bipyridine, LHNa = aniline-2,5-disulfonic acid ......
A Novel Three-dimensional Extended Supramolecular Network Constructed from Octamolybdate Clusters an
A novel organic-inorganic hybrid, Na2(Hmorph)2[Mo8O26]·2H2O(1, Hmorph=morpholine), has been synthesized by convenient a......
Synthesis, Crystal Structure and Properties of a Novel Tetranuclear Nickel(Ⅱ) Complex with Azo-enoli
A novel tetranuclear nickel(Ⅱ) complex [Ni4L2(DMF)2(H2O)2·2DMF] (1,H4L=azo-enolic-2-hydroxybenzamide, DMF=N,N-dimethyl......
Synthesis, Crystal Structure and Luminescence Property of a 2D Mn(Ⅱ) Coordination Polymer Based on I
A novel 2D Mn(Ⅱ) coordination polymer [Mn(CH3COO)2(INH)]n(INH=isoniazid) has been synthesized in DMF solution with ison......
Synthesis and Crystal Structure of a New Cadmium(Ⅱ) Coordination Polymer with Ethylenediaminetetraac
A new cadmium(Ⅱ) coordination polymer,namely,[KCd2(edta)I]n(1,H4edta = ethylenediaminetetraacetic acid),has been prepar......
Synthesis, Crystal Structure and Thermal Stability of a Nickel(Ⅱ) Complex with Bicycle[2.2.1]-2-hept
The nickel complex {Ni(2,2-bipy)(H2O)3[C8H11O2(COO)]}(H2O)3 with bicycle-[2.2.1]-2-hepten-5,6-dicarboxylic acid [C7H8(CO......
Synthesis,Crystal Structure and Anti-tumor Activity of Ethyl 3-(4-methoxyphenyl)-4-oxo-3,3a,4,6-tetr
The title compound(ethyl 3-(4-methoxyphenyl)-4-oxo-3,3a,4,6-tetrahydro-1H-furo[3,4-c]pyran-3a-carboxylate) has been synt......
A new mono-nuclear Mn(Ⅱ) complex [Mn(MPT)2(NCS)(HOCH3)]ClO4(MPT = 2-methoxyl-1,10-phenanthroline) has been synthesized ......
A Two-dimensional Metallic Oxide Constructed from Molybdenum Clusters and Zn(Ⅱ)-[3-(2-pyridyl)pyrazo
A new polyoxomolybdate compound [Zn(HL)2(Mo8O26)(4,4’-Bipy)]·(4,4’-Bipy) (HL = 3-(2-pyridyl)pyrazole, 4,4’-Bipy = 4,......
Two Zinc(Ⅱ) Carboxyarylphosphonates with Unusual Polynuclear Zn(Ⅱ) Units:Syntheses and Crystal Struc
[Zn2(PCP)(phen)(H2O)F]n 1 and {[Zn3(MCP)2(phen)2(H2O)]·2.5H2O}n 2(PCP = p-O2C(C6H4)PO33-,MCP = m-O2C(C6H4)PO33- and phe......
The synthesis and molecular structure of a new dinuclear copper(Ⅰ) complex [Cu(dppb)(NO 3)] 2 are reported.The compound......
Asymmetric Synthesis and Crystal Structure of (-)-N-[(3R)-3-Cyclohexyl]-3-phenylpropananoyl]bornane-
The title compound (-)-N-[(3R)-3-cyclohexyl]-3-phenylpropananoyl]bornane-10,2sultam (C 25 H 35 NO 3 S,M r=429.60),a deri......
Two New Three-dimensional Supramolecular Complexes with 5-Carboxyl-1-carboxymethyl-2-oxidopyridinium
Two new supramolecular complexes [MnL(H2O) 4](1) and [ZnL(H2O) 5]·0.25H2O(2) (H2L = 5-carboxy-1-carboxymethyl-2-oxidopy......
Hydrothermal Synthesis and Crystal Structure of a New 2D Zinc(Ⅱ) Coordination Polymer with 2-Aminoet
A new 2D Zn(Ⅱ) coordination polymer [Zn(TAU)2]n (1, HTAU=2-aminoethane- sulfonic acid) constructed by 2-aminoethanesulf......
Hydrothermal Synthesis, Crystal Structure and Photoluminescent Property of a Novel Complex [Zn(OHCT)
A novel ligand 11-oxa-4,5,9,10,12,13-hexaaza-cyclopenta [b] triphenylene (OHCT) and its coordination polymer [Zn(OHCT)(1......
Syntheses and Crystal Structures of Two New Supramolecular Architectures Constructed from the Main G
The reactions of SbCl3 and HgCl2 with 2-(3-pyridyl)benzimidazole (PyBIm) in solution acidified with HCl have been invest......
Synthesis and Characterization of a Homochrial Manganese(Ⅱ)Complex Constructed from (1R,2R)-(-)-Diam
A homochrial manganese(Ⅱ) complex derived from chiral salen ligand (1R,2R)-(-)diaminocyclohexane-N,N-biscarboxyl-salicy......
The title compound 2-oxo-3-phenyl-1-oxaspiro[4.5]dec-3-en-4-yl 4-chloro-benzoate 6 (C22H19ClO4, Mr = 382.82) has been sy......
Anti-tumor Metastasis and Crystal Structure of N~1-(1,3,4-Thiadiazole-2-yl)-N~3-m-chlorobenzoyl-urea
The title compound N 1-(1,3,4-thiadiazole-2-yl)-N 3-m-chlorobenzoyl-urea (C 9 H 7 N 4 OSCl,M r=254.70) was prepared by t......
A Cu(II) complex of tetra(3,5-diphenyl pyrazole) [Cu(C15H12N2)2Cl2]2 (1) was synthesized, and its structure was determin......
Synthesis and Crystal Structure of 1-(4-Fluorophenyl)-2-hexylthiobenzo[4,5]-furo[3,2-d]-1,2,4-triazo
The crystal structure of the title compound 1-(4-fluorophenyl) -2-hexylthio-benzo [4,5]furo[3,2-d]-1,2,4-triazolo[1,5-a]......
Synthesis,Structure and Physical Properties of Mn and Cd Complexes with 1,1,2,2-Tetracarboxyl-ethyle
Complex [Mn(tce) 0.5(H2O) 4](1) was obtained from Mn(OAc) 2 and tce,where tce is 1,1,2,2-tetracarboxyl-ethane. The struc......